@misc{10481/99302,
year = {2018},
month = {4},
url = {https://hdl.handle.net/10481/99302},
abstract = {Several analytical methods are available to evaluate virgin olive oil (VOO) minor compounds; however, multi-class methodologies are yet rarely studied. Herewith, LC-MS and GC-MS platforms were used to develop two methods capable of simultaneously determine more than 40 compounds belonging to different VOO minor chemical classes within a single run. A non-selective and highly efficient liquid-liquid extraction protocol was optimized for VOO minor components isolation. The separation and detection conditions were adjusted for determining phenolic and triterpenic compounds, free fatty acids and tocopherols by LC-MS, plus sterols and hydrocarbons by GC-MS. Chromatographic analysis times were 31 and 50 min, respectively. A comparative assessment of both methods in terms of analytical performance, easiness, cost and adequacy to the analysis of each class was carried out. The emergence of this kind of multi-class analytical methodology greatly increases throughput and reduces cost, while avoiding the complexity and redundancy of single-chemical class determinations.},
organization = {Spanish Ministry of Economy and Competitiveness (CTQ2014-53442-P)},
organization = {Spanish Ministry of Education, Culture and Sport (FPU13/06438)},
organization = {Mobility Program for young researchers CEI BioTic 2015-2016 (Vice-rectorate for Internationalization of the University of Granada)},
keywords = {virgin olive oil},
keywords = {liquid chromatography},
keywords = {gas chromatography},
keywords = {mass spectrometry},
keywords = {multi-class methodologies},
keywords = {phenolic compounds},
keywords = {pentacyclic triterpenes},
keywords = {tocopherols},
keywords = {sterols},
keywords = {fatty acids},
title = {Deep insight into the minor fraction of virgin olive oil by using LC-MS and GC-MS multi-class methodologies},
doi = {10.1016/j.foodchem.2018.04.006},
author = {Olmo García, Lucía and Polari, Juan J. and Li, Xueqi and Bajoub, Aadil and Fernández Gutiérrez, Alberto and Wang, Selina C. and Carrasco Pancorbo, Alegría},
}